Agilent_1260_液相现场培训手册

点击次数：2759 发布时间：2014/9/11 11:12:05 下载资料

一、目录
二、 培训目的 ........................................................................ 3
三、 培训准备 .......................................................................... 3
1. 仪器准备 .............................................................................. 3
2. 溶剂准备 .......................................................................... 3
四、 方法建立 ......................................................................... 3
1. 开机准备 .......................................................................... 3
2. 数据采集方法编辑 ................................................................... 9

G1310A(单元泵) ........................................................................9

G1312X(二元泵)/G1311X(四元泵) ......................................................... 10

G1313A(标准型自动进样器)，G1329B(自动控温自动进样器) .......................... 11

G1367E(高性能自动进样器) ............................................................. 12

G1328A(手动进样器) ................................................................... 14

G1316A/C (柱温箱) .....................................................................15

G1314BC/E/F(可变波长紫外检测器) ...................................................... 15

G1315C/D ,G4212A/B(二极管阵列检测器)/ G1365C/D(多波长紫外检测器) ..................... 17

G1362A(示差检测器) .................................................................... 18

G1321A(荧光检测器) ..................................................................... 19

G4218A(蒸发光散射检测器) ................................................................. 21
3. 数据分析方法编辑 .................................................................... 22

谱图优化 ................................................................................. 22

积分参数优化 ............................................................................ 23

校正 ..................................................................................... 25

打印报告 ................................................................................ 27

光谱 ....................................................................................28
4. 建立全新完整方法向导................................................................. 30
5. 进样 ................................................................................... 30

单针进样 .................................................................................. 30

序列进样 ................................................................................. 31
五、 关机......................................................................................... 33
1. 关闭检测器的灯 ............................................................................... 33
2. 冲洗系统 ....................................................................................... 33
3. 封存色谱柱 ......................................................................................... 33
4. 关闭电脑 ...................................................................................... 33
5. 关闭模块 .......................................................................................... 33
六、 RRLC(快速液相)注意事项 ............................................................ 33
七、 特殊检测器的注意事项........................................................................... 35
八、 Agilent 1260 常见问题解决方法 ..................................................... 37
附一、 维护知识 ....................................................................................... 39
附二、 注册OpenLAB CDS 许可证的流程 .............................................. 41