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安捷伦1260II高效液相色谱仪

1
仪器介绍

 Agilent 1260 Infinity II 液相色谱系统 与最新色谱柱技术和先进的备件相结合,可保证稳定可靠的分离和检测性能。1260 Infinity II 四元泵能够提供高达 600 bar 的压力,完美适用于InfinityLab Poroshell 120 色谱柱。无脉冲、稳定而混合均匀的梯度可确保获得更高的灵敏度和更可靠的结果,而较小的填料颗粒可实现更快速的分离和更高的分离度。这款泵最多支持四种溶剂,使您在自动溶剂混合中获得极高灵活性,适用于各种研究和常规应用。稳定的材料能够耐受最苛刻的应用,能够支持泵持续运行数年,从而最大程度缩短停机时间并降低运行成本。 在分析生物样品或需要采用极端 pH 条件的应用中,可采用高度耐腐蚀的钛金属四元泵。与其他 1260 Infinity II 生物惰性模块结合后,即可配置出安捷伦独有的包含完全无金属样品流路、且压力范围高达 600 bar 的系统。 1260 Infinity II 高容量柱温箱最多可容纳四根 30 cm 色谱柱,并可通过 InfinityLab 快速更换切换阀直接操作每根色谱柱。无需断开并重新连接色谱柱即可自动运行不同方法。全部四根色谱柱均包含的固定式标签可记录色谱柱 ID 和完整使用历史,确保符合法规指南要求。色谱柱追踪也有助于避免重要序列运行过程中的故障,或避免固定相、溶剂和温度不匹配。 二极管阵列检测器的高灵敏度流通池能够检测极低的样品浓度。我们还为二极管阵列检测器和荧光检测器提供了特殊的生物惰性流通池,确保对生物样品实现安全的数据采集。

2
指标

 Physical Specifications Agilent 1260 Infinity II Isocratic Pump(G7110B)

安捷伦1260ⅡG7110B等度泵

 

Type

Specification

Comments

Weight

14.7 kg (32 lbs)

 

Dimensions

(height × width × depth)

180 x 396 x 436 mm

(7.1 x 15.6 x 17.2 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

80 VA, 65 W

 

Ambient operating

temperature

455 °C (39131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 Physical Specifications Agilent 1260 Infinity II Quaternary Pump VL

(G7111A)

Table 2 Physical Specifications

Type

Specification

Comments

Weight

14.7 kg (32 lbs)

 

Dimensions

(height × width × depth

180 x 396 x 436 mm

(7.1 x 15.6 x 17.2 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

80 VA, 65 W

 

Ambient operating

temperature

455 °C (39131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 Physical Specifications Agilent 1260 Infinity II Quaternary Pump

(G7111B)

Table 3 Physical Specifications

Type

Specification

Comments

Weight

14.7 kg (32 lbs)

 

Dimensions

(height × width × depth)

180 x 396 x 436 mm

(7.1 x 15.6 x 17.2 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

80 VA, 65 W

 

Ambient operating

temperature

455 °C (39131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

Physical Specifications Agilent 1260 Infinity II -G7102A Physical Specifications

Type

Specification

Comments

Weight

11 kg (non-cooled), 13 kg (cooled)

 

Dimensions

(height × width × depth)

415 x 200 x 450 mm

(16.3 x 7.9 x 17.7 inches)

 

Line voltage

100 – 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

150 W (max)

Maximum

Ambient operating

temperature

10–35 °C (50–95 °F)

 

Ambient non-operating

temperature

-40 – 70 °C (-40 – 158 °F)

 

Humidity

< 80 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 2000 m (6562 ft)

 

Non-operating altitude

Up to 4600 m (15091 ft)

For storing the module

Safety standards:

IEC, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

 

Performance Specification of the ELS Detector

Type

Specification

Light Source

 

G7102A

LASER 405 nm, 10 mW (Class 3B)

Detector

Dual PMT with digital signal processing

Nebuliser

OFF, 25 – 90 °C

Evaporator

 

Non-cooled

OFF, 25 – 120 °C

Cooled

OFF, 10 – 80 °C

Gas Flow Range

0.9 – 3.25 SLM (controlled gas shut-off)

Short Term Noise

<0.1 mV under specified condtions. See “Specification

Conditions” on page 24.

Drift

<1 mV/h under specified condtions. See “Specification

Conditions” on page 24.

Operating Pressure

60 – 100 psi (4.1 – 6.9 bar)

Eluent Flow range

0.2 – 5.0 mL/min

Digital Output

10, 40 or 80 Hz (24 bit)

 G7114B  Physical Specifications

Type

Specification

Comments

Weight

11 kg (24.3 lbs)

 

Dimensions

(height × width × depth)

140 x 396 x 436 mm

(5.5 x 15.6 x 17.2 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

80 VA, 70 W

 

Ambient operating

temperature

4 - 55 °C (39 - 131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

 Agilent 1260 Infinity II Variable Wavelength Detector (G7114A) Performance Specifications

 

Feature

Specification

Detection type

Double-beam photometer

Light source

Deuterium lamp

Number of signals

Single and dual wavelength detection

Maximum data rate

120 Hz (single wavelength detection)

2.5 Hz (dual wavelength detection)

Noise

<±0.25·10-5 AU, at 230 nm (single wavelength detection)

<±0.80·10-5 AU, at 230 nm and 254 nm (dual wavelength detection)

Drift

<1·10-4 AU/h, at 230 nm

Linearity

>2.5 AU upper limit

Wavelength range

190 600 nm

Wavelength

accuracy

±1 nm, self-calibration with deuterium lines, verification with holmium

oxide filter

Wavelength

precision

<±0.1 nm

Slit width

6.5 nm typical over whole wavelength range

Time programmable

Wavelength, polarity, peak width, lamp on/off

Flow cells

Standard: 14 μL volume, 10 mm cell path length and 40 bar (588 psi)

pressure maximum

Micro: 2 μL volume, 3 mm cell path length and 120 bar (1760 psi) pressure

maximum

Semi-micro: 5 μL volume, 6 mm cell path length and 40 bar (588 psi)

pressure maximum

Preparative: 4 μL volume, 3 mm cell path length and 120 bar (1760 psi)

pressure maximum

Preparative: 0.3 mm cell path length and 50 bar (725 psi) pressure

maximum

Preparative: 0.06 mm cell path length and 50 bar (725 psi) pressure

maximum

High pressure: 14 μL volume, 10 mm cell path length and 400 bar

(5801 psi) pressure maximum

Spectral tools

Stop-flow wavelength scan

Analog output

Recorder/Integrator 100 mV or 1 V, 1 output

Communication

LAN, Controller-area network (CAN),

ERI: ready, start, stop and shut-down signals,

USB

GLP

Early maintenance feedback (EMF) for continuous tracking of instrument

usage in terms of lamp burn time with user settable limits and feedback

messages. Electronic records of maintenance and errors. RFID for

electronics records of flow cell and UV lamp conditions (path length,

volume, product number, serial number, test passed, and usage).

Verification of wavelength accuracy with built-in holmium oxide filter.

Safety and

maintenance

Extensive diagnostics, error detection and display through Agilent Instant

Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling,

leak output signal for shutdown of pumping system. Low voltages in

major maintenance areas. Tracking of flow cells and lamps with RFID

(radio frequency identification) tags

 

 Physical Specifications G7115A

 

Type

Specification

Comments

Weight

12 kg (26.5 lbs)

 

Dimensions

(height × width × depth)

140 x 396 x 436 mm

(5.5 x 15.6 x 17 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

110 VA / 100 W

 

Ambient operating

temperature

455 °C (39131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

 

Performance Specifications G7115A

Type

Specification

Comments

Detection type

1024-element photodiode array

 

Light source

Deuterium and tungsten lamps

The UV-lamp is equipped with

RFID tag that holds lamp typical

information.

Data rate

up to 120 Hz

 

Wavelength range

190 – 950 nm

 

Short term noise

(ASTM) Single and

Multi-Wavelength

< ± 0.7·10-5 AU at 254 and 750 nm

see "Specification Conditions"

below

Drift

< 0.9·10-3 AU/h at 254 nm

see "Specification Conditions"

below

Linear absorbance

range

> 2 AU (5 %) at 265 nm

see "Specification Conditions"

below

Wavelength

accuracy

± 1 nm

Self-calibration with deuterium

lines, verification with holmium

oxide filter

Wavelength

bunching

1 – 400 nm

Programmable in steps of 1 nm

Slit width

1, 2, 4 , 8, 16 nm

Programmable slit

Diode width

< 1 nm

 

Flow cells

Standard: 13 μL volume, 10 mm cell

path length and 120 bar (1740 psi)

pressure maximum

Standard bio-inert: 13 μL volume,

10 mm cell path length and 120 bar

(1740 psi) pressure maximum

Semi-micro: 5 μL volume, 6 mm cell

path length and 120 bar (1740 psi)

pressure maximum

Micro: 2 μL volume, 3 mm cell path

length, 120 bar (1740 psi) pressure

maximum

Semi-nano: 500 nL volume, 10 mm

cell path length and 50 bar (725 psi)

pressure maximum

Nano: 80 nL volume, 6 mm cell path

length and 50 bar (725 psi) pressure

maximum

High pressure: 1.7 μL volume, 6 mm

cell path length and 400 bar

(5800 psi) pressure maximum

Prep SST: 3 mm cell path length and

120 bar (1740 psi) pressure maximum

Prep Quartz:0.3 mm cell path length

and 20 bar (290 psi) pressure

maximum

Prep Quartz: 0.06 mm cell path length

and 20 bar (290 psi) pressure

maximum

All flow cells are equipped with

RFID tags that hold cell typical

information.

pH range 1.0 – 9.5 (12.5 solvent

dependent with bio-inert version

Time programmable

Wavelength, polarity, peak width,

lamp bandwidth, autobalance,

wavelength range, threshold, spectra

storage mode

 

Spectral tools

Data analysis software for spectra

evaluation, including spectral

libraries and peak purity functions

 

Control and data

evaluation

Agilent OpenLab CDS

OpenLab CS C.01.07

Driver A.02.14

 

 Agilent 1260 Infinity II Variable Wavelength Detector (G7116A) Physical Specifications

 

Type

Specification

Comments

Weight

12.5 kg (27.6 lbs)

 

Dimensions

(height × width × depth)

160 x 435 (472*) x 436 mm (6.3 x 17.1

(18.6*) x 17.2 inches) *with column ID kit

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

150 VA, 150 W

 

Ambient operating

temperature

455 °C (39131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

Agilent 1260 Infinity II Multicolumn Thermostat (G7116A) Performance Specifications

Feature

Specification1

Operating principle

Thermostatted column compartment with dual, independent

Peltier-element. Solvent pre-heating and still-air operation for reduction of

chromatographic band-broadening under UHPLC-conditions.

Temperature range

10 °C below ambient (minimum 4 °C) to 85 °C settable in steps of 0.1 K

Temperature stability

±0.1 °C

Temperature

accuracy

±0.5 °C (with calibration for 40 °C)

Temperature

precision

0.05 °C

Independent

Temperature zones

2in single device

Column capacity

4 columns of up to 300 mm length plus A-Line Quick-Connect fittings or

pre-column

Number of pre column Quick-Connect Heat Exchangers is scalable each

column can be equipped with individual heat exchanger for best

performance

4-column selector valve is available to access each column without

replumbing

Heat-up/cool-down

time

5 min from ambient to 40 °C

10 min from 40 °C to 20 °C

<25 min from 25 °C to 85 °C

Solvent heat

exchangers

For pre-column solvent heating, G7116A is equipped with a

Quick-Connect Heat Exchanger Large ID (0.17 mm capillary, 3 μL internal

volume) as default.

Other dimensions of Quick-Connect Heat Exchangers are optionally

available as well as heat exchangers made out of bio-inert materials

(metal-free).

Valve options

1 x integrated valve drive as option

to host user-exchangeable Quick-Change valve heads (up to 600 bar) of

different formats:

2-position/6-port, 2-position/10-port, 4-column selection.

Also available in bio-inert materials.

Valve heads are automatically identified by their tag.

Column identification

Optionally, column identification kit to track history of up to four columns.

Mounted left hand-side of module.

Communications

Controller-area network (CAN).

G7116A is a hosted module (LC stack needs to contain a LAN

communication and control card)

Software

compatibility

Requires

OpenLAB CDS A.01.03 - A.02.02 (with LC & CE Drivers A.02.14)

?penLAB CDS ChemStation ed. C.01.03 -C.01.07 SR2 or higher

?OpenLAB CDS EZChrom ed. A.04.05 - A.04.07 SR2 or higher

MassHunter (LC Drivers A.02.14)

?MassHunter B.07.01 or higher for (Q)-TOF

?MassHunter B.08.02 or higher for QQQ

Safety and

maintenance

Extensive diagnostics, error detection and display (through Instant Pilot

control module and Agilent LabAdvisor), leak detection, safe leak

handling, leak output signal for shutdown of pumping system. Low

voltages in main maintenance areas.

GLP

Valve heads carrying tags with serial number, pressure rating, number of

switches and valve type.

Concept of column identification.

 Agilent 1260 Infinity II Variable Wavelength Detector (G7117A) Physical Specifications

Type

Specification

Comments

Weight

11.5 kg (25.4 lbs)

 

Dimensions

(height × width × depth)

140 x 396 x 436 mm

(5.5 x 15.6 x 17.2 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

110 VA, 100 W

 

Ambient operating

temperature

4 40 °C (39 104 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

 

 

 

Agilent 1260 Infinity II Variable Wavelength Detector (G7117A) Performance Specifications

 

Feature

Specification

Detector type

1024-element diode array

Light source

Deuterium

Number of signals

8

Maximum sampling

rate

120 Hz (both spectra and signals)

Short-term noise

with 10 mm Max-Light cartridge cell: <±3·10-6 AU at 230/4 nm, slit width

4 nm, TC 2 s, ASTM

with 60 mm Max-Light cartridge cell: <±0.6·10-6 AU/cm at 230/4 nm, slit

width 4 nm, TC 2 s, ASTM

Drift

<0.5·10-3 AU/h at 230 nm

Linearity

>2.0 AU (5 %) at 265 nm

Typically 2.5 AU (5 %)

Wavelength range

190 640 nm

Wavelength

accuracy

±1 nm, self-calibration with deuterium lines

Wavelength

precision

<±0.1 nm

Diode width

~0.5 nm

Wavelength

bunching

Programmable, 2 400 nm, in steps of 1 nm

Flow cells

User-exchangeable, self-aligning cartridge cells with RFID tags.

Max-Light Cartridge Cell (Standard): 10 mm, σV = 1.0 μL

Max-Light Cartridge Cell (High Sensitivity): 60 mm, σV = 4 μL

Max-Light Cartridge Ultra Low Dispersion (ULD) Cell: 10 mm, σV = 0.6 μL

Max-Light Cartridge High Dynamic Range (HDR) Cell: 3.7 mm, σV = 0.8 μL

Maximum Operating Pressure (MOP)1: 70 bar

Maximum Incidental Pressure (MIP)2: 150 bar

Spectral tools

Data analysis software for spectra evaluation, including spectral libraries

and peak purity functions

Analog output

Recorder/integrator: 100 mV or 1 V, output range 0.001 2 AU, one

outpu

Communications

LAN, controller-area network (CAN),

ERI: ready, start, stop and shut-down signals

USB

GLP features

RFID for electronics records of flow cell and UV lamp conditions (path

length, volume, product number, serial number, test passed, usage)

Early maintenance feedback (EMF) for continuous tracking of instrument

usage in terms of lamp burn time with user settable limits and feedback

messages. Electronic records of maintenance and errors. Verification of

wavelength accuracy with deuterium lines.

Safety and

maintenance

Extensive diagnostics, error detection and display through Agilent Instant

Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling,

leak output signal for shutdown of pumping system. Low voltages in

major maintenance areas.

Others

Second generation of Electronic temperature control (ETC) for the

complete optical unit

 

 

 Agilent 1290 Infinity II Diode Array Detector (G7117B) Performance Specifications

 

Feature

Specification

Detector type

1024-element diode array

Light source

Deuterium

Number of signals

8

Maximum sampling

rate

240 Hz (both spectra and signals)

Short-term noise

with 10 mm Max-Light cartridge cell: <±3·10-6 AU at 230/4 nm, slit width

4 nm, TC 2 s, ASTM

with 60 mm Max-Light cartridge cell: <±0.6·10-6 AU/cm at 230/4 nm, slit

width 4 nm, TC 2 s, ASTM

Drift

<0.5·10-3 AU/h at 230 nm

Linearity

>2.0 AU (5 %) at 265 nm

Typically 2.5 AU (5 %)

Wavelength range

190 640 nm

Wavelength

accuracy

±1 nm, self-calibration with deuterium lines

Wavelength

precision

<±0.1 nm

Slit width

Programmable: 1, 2, 4, 8 nm

Diode width

~0.5 nm

Wavelength

bunching

Programmable, 2 400 nm, in steps of 1 nm

Spectral tools

Data analysis software for spectra evaluation, including spectral libraries

and peak purity functions

Flow cells

User-exchangeable, self-aligning cartridge cells with RFID tags.

Max-Light Cartridge Cell (Standard): 10 mm, σV = 1.0 μL

Max-Light Cartridge Cell (High Sensitivity): 60 mm, σV = 4 μL

Max-Light Cartridge Ultra Low Dispersion (ULD) Cell: 10 mm, σV = 0.6 μL

Max-Light Cartridge High Dynamic Range (HDR) Cell: 3.7 mm, σV = 0.8 μL

Maximum Operating Pressure (MOP)1: 70 bar

Maximum Incidental Pressure (MIP)2: 150 bar

Analog output

Recorder/integrator: 100 mV or 1 V, output range 0.001 – 2 AU, one

output

Communications

LAN, controller-area network (CAN),

ERI: ready, start, stop and shut-down signals,

USB

GLP features

RFID for electronics records of flow cell and UV lamp conditions (path

length, volume, product number, serial number, test passed, usage)

Early maintenance feedback (EMF) for continuous tracking of instrument

usage in terms of lamp burn time with user settable limits and feedback

messages. Electronic records of maintenance and errors. Verification of

wavelength accuracy with deuterium lines.

Safety and

maintenance

Extensive diagnostics, error detection and display through Agilent Instant

Pilot and Agilent Lab Advisor software. Leak detection, safe leak handling,

leak output signal for shutdown of pumping system. Low voltages in

major maintenance areas.

Others

Second generation of Electronic temperature control (ETC) for the

complete optical unit

 Agilent 1290 Infinity II High Speed Pump (G7120A)  Physical Specifications

Type

Specification

Comments

Weight

21.0 kg (46.3 lbs)

 

Dimensions

(height × width × depth)

200 x 396 x 436 mm

(7.9 x 15.6 x 17.2 inches)

 

Line voltage

100 – 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

210 VA / 180 W

 

Ambient operating

temperature

4 – 55 °C (39 – 131 °F)

 

Ambient non-operating

temperature

-40 – 70 °C (-40 – 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

 

Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications

Feature

Specification

Hydraulic system

Two dual pistons in series, pumps with proprietary servo-controlled

variable stroke design and smooth motion control.

Pump resolution step

size

300 pL step size

Settable flow range

0.001 – 5 mL/min, in 0.001 mL/min increments (executed in 300 pL/step

increments).

Flow precision

≤0.07 % RSD or 0.005 min SD, whatever is greater

Flow accuracy

±1 % or 10 μL/min, whatever is greater

Pressure range

up to 130 MPa (1300 bar) at 0 – 2 mL/min

ramping down to 80 MPa (800 bar) at 5 mL/min

Pressure pulsation

<1 % amplitude or <0.5 MPa (5 bar), whatever is greater

Compressibility

compensation

Automatic

Recommended

pH-range

1.0 – 12.5, solvents with pH <2.3 should not contain acid which attack

stainless steel.

Gradient formation

High pressure binary mixing

Delay volume

As low as 45 μL (10 μL without mixer)

Composition

precision

<0.15 % RSD or 0.01 min SD, whatever is greater

Composition

accuracy

±0.35 % absolute

Number of solvent

2 out of maximum 26 solvents

Solvent selection

valve

Internal 4-solvent selection valve included.

External 2x 12 solvent valve as option, fully integrated in the pump control

interface.

 Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications

Feature

Specification

Hydraulic system

Two dual pistons in series, pumps with proprietary servo-controlled

variable stroke design and smooth motion control.

Pump resolution step

size

300 pL step size

Settable flow range

0.001 – 5 mL/min, in 0.001 mL/min increments (executed in 300 pL/step

increments).

Flow precision

≤0.07 % RSD or 0.005 min SD, whatever is greater

Flow accuracy

±1 % or 10 μL/min, whatever is greater

Pressure range

up to 130 MPa (1300 bar) at 0 – 2 mL/min

ramping down to 80 MPa (800 bar) at 5 mL/min

Pressure pulsation

<1 % amplitude or <0.5 MPa (5 bar), whatever is greater

Compressibility

compensation

Automatic

Recommended

pH-range

1.0 – 12.5, solvents with pH <2.3 should not contain acid which attack

stainless steel.

Gradient formation

High pressure binary mixing

Delay volume

As low as 45 μL (10 μL without mixer)

Composition

precision

<0.15 % RSD or 0.01 min SD, whatever is greater

Composition

accuracy

±0.35 % absolute

Number of solvent

2 out of maximum 26 solvents

Solvent selection

valve

Internal 4-solvent selection valve included.

External 2x 12 solvent valve as option, fully integrated in the pump control

interface.

Type

Specification

 

Weight

11.9 kg (26.2 lbs)

 

Dimensions

(height × width × depth)

140 x 396 x 436 mm

(5.5 x 15.6 x 17.0 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

70 VA, 60 W

 

Ambient operating

temperature

4-55 °C (39-131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 G7121A Physical Specifications

Type

Specification

 

Weight

11.9 kg (26.2 lbs)

 

Dimensions

(height × width × depth)

140 x 396 x 436 mm

(5.5 x 15.6 x 17.0 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

70 VA, 60 W

 

Ambient operating

temperature

4-55 °C (39-131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

 

Performance Specifications Agilent 1260 Infinity II Fluorescence Detector

SPECTRA (G7121B)

Type

Specification

Comments

Detection type

Multi-signal fluorescence detector with

rapid on-line scanning capabilities and

spectral data analysis

 

Performance specifications

Single wavelength operation:

RAMAN (H2O) > 500 (noise reference

measured at signal)

Ex=350 nm, Em=397 nm, dark value

450 nm, standard flow cell

RAMAN (H2O) > 3000 (noise

reference measured at dark value)

Ex=350 nm, Em=397 nm, dark value

450 nm, standard flow cell

Dual wavelength operation:

RAMAN (H2O) > 300 Ex 350 nm, Em

397 nm and Ex 350 nm, Em 450 nm,

standard flow cell.

Reference conditions:

Standard cell 8 μL,

response time 4 s,

HPLC-grade water and

restriction capillary.

For details refer to the

Service Manual.

Light source

Xenon Flash Lamp, normal mode 20 W,

economy mode 5 W, lifetime 4000 h

 

Pulse frequency

296 Hz for single signal mode

74 Hz for economy mode

 

Maximum data rate

74 Hz, 148 Hz

 

Excitation monochromator

Range: settable 200 nm - 1200 nm and

zero-order

Bandwidth: 20 nm (fixed)

Monochromator: concave holographic

grating, F/1.6, blaze: 300 nm

 

Emission monochromator

Range: settable 200 nm - 1200 nm and

zero-order

Bandwidth: 20 nm (fixed)

Monochromator: concave holographic

grating, F/1.6, blaze: 400 nm

 

Reference system

in-line excitation measurement

 

Timetable programing

up to 4 signal wavelengths, response

time, PMT Gain, baseline behavior

(append, free, zero), spectral parameters

 

Spectrum acquisition

Excitation or Emission spectra

Scan speed: 28 ms per datapoint (e.g.

0.6 s/spectrum 200 400 nm, 10 nm

step)

Step size: 1 20 nm

Spectra storage: All

 

Wavelength characteristic

Repeatability +/- 0.2 nm

Accuracy +/- 3 nm setting

 

Flow cells

Standard: 8 μL volume and 20 bar

(2 MPa) pressure maximum, fused silica

block

Optional:

Bio-inert: 8 μL volume and 20 bar

(2 MPa) pressure maximum, (pH

112)

Micro: 4 μL volume and 20 bar

(2 MPa) pressure maximum

 

Control and data evaluation

Agilent ChemStation for LC, Agilent

Instant Pilot G4208A with limited spectral

data analysis and printing of spectra

 

 G7129AB Physical Specifications

 

Type

Specification

Comments

Weight

19 kg (41.9 lbs)

w/o sample cooler

Dimensions

(height × width × depth)

324 x 396 x 468 mm

(12.8 x 15.6 x 18.4 inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

350 VA / 350 W / 1195 BTU/h

 

Ambient operating

temperature

4 - 40 °C (39 - 104 °F), without chiller up

to 55 °C (131 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)1

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

Permitted solvents

Boiling point ≥56 °C

Auto-ignition temperature ≥200 °C

 

 

 

 

Performance Specifications (G7129A)

Type

Specification

Comment

Injection range

0.1 100 μL in 0.1 μL increments with 100 μL

up to 60 MPa

0.1 900 μL in 0.1 μL increments with 900 μL

up to 40 MPa

Up to 1800 μL with multiple draw (hardware

modification required)

Requires 900 μL analytical head

Precision

<0.25 % RSD of peak areas from <5 μL to

100 μL

Measured caffeine

Pressure range

0 60 MPa (0 600 bar, 0 8702 psi)

0 40 MPa (0 400 bar, 0 5801 psi)

for 900 μL Analytical Head

Sample viscosity

range

0.2 5 cp

 

Sample capacity

132 x 2 mL vial (two trays default)

100 x 2 mL vial (two classic trays optional)

36 x 6 mL vials (two trays optional)

 

Carry over

<0.004 % (40 ppm) with needle wash

Using the following conditions:

ZORBAX Eclipse Plus C18, RRHD, 2.1 x 50

mm, 1.8 μm (959757-902)

Mobile Phase:

A: 0.1 % TFA in water

B: 0.1 % TFA in acetonitrile

Isocratic : % B=33 %

Flow rate: 0.5 mL/min

Column temperature: 50 °C

Wavelength detection: 257/4 nm, ref.

wavelength 380/100 nm, 20 Hz

Injection volume: 1 μL

Sample: 1200 ng/μL Chlorhexidine for UV,

(dissolved with mobile phase A), 1 μL

injected and measured both on Agilent

G7117B DAD

Wash solution: H2O with 0.1 % TFA (5 s)

Injection cycle time

18 s for draw speed 200 μL/min

Ejection speed: 200 μL/min

Injection volume: 1 μL

 

Minimum sample

volume

1 μL from 5 μL sample in 100 μL microvial, or

1 μL from 10 μL sample in 300 μL microvial.

Needle height offset has to be adapted to

ensure that needle doesnt touch vial bottom.

Default needle height = 0 equates to 2 mm

above the vial bottom.

Control and data

evaluation

Agilent OpenLab CDS

MassHunter QQQ

MassHunter TOF/QTOF

Lab Advisor

ICF for 3rd party SW control

LC and CE Drivers

A.02.02 or above

B.08.01 or above

B.07.02 or above

B.02.07 or above

A.02.04 or above

A.02.12 or above

Local control

Agilent Instant Pilot (G4208A)

B.02.17 or above

Communications

Controller-area network (CAN),Local Area

Network (LAN)

ERI: ready, start, stop and shut-down signals

 

Safety and

maintenance

Extensive support for troubleshooting and

maintenance is provided by the Instant Pilot,

Agilent Lab Advisor, and the Chromatography

Data System. Safety-related features are leak

detection, safe leak handling, leak output signal

for shutdown of pumping system, and low

voltages in major maintenance areas.

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage with

user-settable limits and feedback messages.

Electronic records of maintenance and errors

 

Housing

All materials recyclable.

 

Metering device

Metering device in high pressure flow path

 

 

 

Performance Specifications (G7129B)

Type

Specification

Comment

Injection range

0.1 20 μL in 0.1 μL increments (default)

0.1 40 μL in 0.1 μL increments if 40 μL loop is

installed

0.1 120 μL in 0.1 μL increments with 1290

Infinity large volume injection kit (hardware

modification required)

0.1 100 μL in 0.1 μL (if 100 μL-loop and

100 μL-head is installed)

Up to 1500 μL with 1400 μL-multi-draw kit and

100 μL-analytical head

up to 130 MPa (1300 bar, 18854 psi)

up to 60 MPa (600 bar, 8702 psi)

Precision

<0.25 % RSD of peak areas from 5 μL to 100 μL

Measured caffeine

Pressure range

Up to 130 MPa (1300 bar, 18854 psi)

 

Sample viscosity

range

0.2 5 cp

 

Sample capacity

132 x 2 mL vial (two trays default)

100 x 2 mL vial (two classic trays optional)

36 x 6 mL vials (two trays optional)

 

Carry over

<0.004 % (40 ppm) with needle wash

Using the following conditions:

ZORBAX Eclipse Plus C18, RRHD, 2.1 x 50

mm, 1.8 μm (959757-902)

Mobile Phase:

A: 0.1 % TFA in water

B: 0.1 % TFA in acetonitrile

Isocratic : % B=33 %

Flow rate: 0.5 mL/min

Column temperature: 50 °C

Wavelength detection: 257/4 nm, ref.

wavelength 380/100 nm, 20 Hz

Injection volume: 1 μL

Sample: 1200 ng/μL Chlorhexidine for UV,

(dissolved with mobile phase A), 1 μL

injected and measured both on Agilent

G7117B DAD

Wash solution: H2O with 0.1 % TFA (5 s)

Injection cycle time

18 s for draw speed 200 μL/min

Ejection speed: 200 μL/min

Injection volume: 1 μL

 

Minimum sample

volume

1 μL from 5 μL sample in 100 μL microvial, or

1 μL from 10 μL sample in 300 μL microvial.

Needle height offset has to be adapted to

ensure that needle doesnt touch vial bottom.

Default needle height = 0 equates to 2 mm

above the vial bottom.

Control and data

evaluation

Agilent OpenLab CDS

MassHunter QQQ

MassHunter TOF/QTOF

Lab Advisor

ICF for 3rd party SW control

LC and CE Drivers

A.02.02 or above

B.08.01 or above

B.07.02 or above

B.02.07 or above

A.02.04 or above

A.02.12 or above

Local control

Agilent Instant Pilot (G4208A)

B.02.17 or above

Communications

Controller-area network (CAN),Local Area

Network (LAN)

ERI: ready, start, stop and shut-down signals

 

Safety and

maintenance

Extensive support for troubleshooting and

maintenance is provided by the Instant Pilot,

Agilent Lab Advisor, and the Chromatography

Data System. Safety-related features are leak

detection, safe leak handling, leak output signal

for shutdown of pumping system, and low

voltages in major maintenance areas.

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage with

user-settable limits and feedback messages.

Electronic records of maintenance and errors.

 

Housing

All materials recyclable.

 

Metering device

Metering device in high pressure flow path

 

 

 Physical Specifications G7162A

 

Type

Specification

Comments

Weight

15 kg (33 lbs)

 

Dimensions

(height × width × depth)

180 x 396 x 436 mm

(7.1 x 15.6 x 17.2 inches)

 

Line voltage

100 – 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

70 W / 80 VA

 

Ambient operating

temperature

4–55 °C (39–131 °F)

 

Ambient non-operating

temperature

-40 – 70 °C (-40 – 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

 

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

 

 

 

Physical Specifications Agilent 1260 Infinity II Multisampler

(G7167B)

Type

Specification

Comments

Weight

22 kg (48.5 lbs)

w/o sample cooler

Dimensions

(height × width × depth)

320 x 396 x 468 mm (12.6 x 15.6 x 18.4

inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

180 VA, 180 W

 

Ambient operating

temperature

4 - 40 °C (39 - 104 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

Permitted solvents

Boiling point ≥56 °C

Auto-ignition temperature ≥200 °C

 

 

Physical Specifications Agilent 1260 Infinity II Bio-inert

Multisampler (G5668A)

Type

Specification

Comments

Weight

22 kg (48.5 lbs)

w/o sample cooler

Dimensions

(height × width × depth)

320 x 396 x 468 mm (12.6 x 15.6 x 18.4

inches)

 

Line voltage

100 240 V~, ± 10 %

Wide-ranging

capability

Line frequency

50 or 60 Hz, ± 5 %

 

Power consumption

180 VA, 180 W

 

Ambient operating

temperature

4 - 40 °C (39 - 104 °F)

 

Ambient non-operating

temperature

-40 70 °C (-40 158 °F)

 

Humidity

< 95 % r.h. at 40 °C (104 °F)

Non-condensing

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15092 ft)

For storing the module

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

Permitted solvents

Boiling point ≥56 °C

Auto-ignition temperature ≥200 °C

 

 

 Table 3 Agilent 1290 Infinity II Multisampler (G7167B) Performance Specifications

Type

Specification

Comment

Injection range for

Single-needle

instruments

Default: 0.1 20 μL in 0.1 μL increments;

optional: 40 μL or 100 μL (using 100 μL analytical

head)

Up to 1300 bar using 40 μL (default) or

optional 100 μL analytical head

 

Pressure range up to 400 bar due to 900 μL

analytical head

Pressure range up to 400 bar due to 900 μL

analytical head

 

0.1 500 μL or 900 μL in 0.1 μL increments (using

900 μL analytical head)

Pressure range up to 1300 bar Multi-draw

modus (Injection into needle-seat capillary

Injection range for

Dual-needle

instruments

Default: 0.1 20 μL in 0.1 μL increments;

optional: 40 μL or 100 μL

Up to 1300 bar using 100 μL analytical head

 

Up to 500 μL in 0.1 μL increments depending on

installed loop size

Up to 1300 bar using 100 μL analytical head +

Multi-load

Precision for

Single-needle

instruments

<0.15 % RSD or SD <10 nL, whatever is greater

Measured caffeine

Precision for

Dual-needle

instruments

<0.2 % RSD or SD <10 nL, whatever is greater

Measured caffeine

Pressure range

Up to 1300 bar (G7167B)

Max pressure for basic instrume

Sample viscosity

range

0.2 5 cp

Max. 6144/1536 samples (384MTP/96)

Sample capacity

1H Drawer up to 8 drawers and 16 positions

Shallow well plates (MTP)

3072 samples, 432 vials (2 mL)

 

2H Drawer up to 4 drawers and 8 positions

MTP, deep well plates, vials, Eppendorf

1536 samples, 60 vials (6 mL), 384 vials

(1 mL), 216 vials (2 mL)

 

3H Drawer up to 2 drawers and 4 positions

MTP, deep well plates, vials up to 6 mL,

Eppendorf

Using standard Single-needle setup

 

 

Time between 2 injections is not

mechanically limited, time delay depends on

communication speed of software, OS or

network connections

Carry Over

<0.003 % (30 ppm) Multisampler Standard and

Dual Needle

<0.0009 % (9 ppm) Multisampler Multiwash

Using the following conditions:

Column: Agilent Pursuit XRs 3 C18, 2.0 x

50 mm

Mobile phase:

A: 0.1 % TFA in water

B: 0.1 % TFA in Acetonitrile

Isocratic : % B=40 %

Flow rate: 0.5 mL/min

Temperature: 25 °C

Wavelength: 257 nm

Sample: 1200 ng/μL Chlorhexidine

(dissolved with mobile phase A), 1 μL

injected and measured on G4212A DAD

Wash solution: H2O with 0.1 % TFA (3 s)

Multiwash

Outer needle wash and seat backflush for

carryover reduction with up to 3 different

solvents

 

Control and data

evaluation

Agilent Open Lab CDS

A.02.01 or above (A.02.02 supports Sample

Entry UI)

 

MassHunter QQQ

B.07.00 SP11 or above

 

MassHunter QTOF

B.05.01 SP31 or above

 

Lab Advisor

B.02.05 or above

 

ICF for 3rd party SW control

A.02.01 or above

 

LC and CE Drivers

A.02.10 or above

Local Control

Agilent Instant Pilot (G4208A)

B.02.17 or above (currently not

supported/official release 2015)

Communications

Controller-area network (CAN), Local Area

Network (LAN)

ERI: ready, start, stop and shut-down signals

 

Safety and

maintenance

Extensive support for troubleshooting and

maintenance is provided by the Instant Pilot,

Agilent Lab Advisor, and the Chromatography

Data System.

Safety-related features are leak detection, safe

leak handling, leak output signal for shutdown of

pumping system, and low voltages in major

maintenance areas.

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage with

user-settable limits and feedback messages.

Electronic records of maintenance and errors

 

Housing

All materials recyclable

 

Metering device

Metering device in high pressure flow path

 

Performance Specifications (G7167A)

Table 4 Agilent 1260 Infinity Multisampler (G7167A) Performance Specifications

 

Type

Specification

Comment

Injection range for

Single-needle

instruments

Default: 0.1 100 μL in 0.1 μL increments;

optional: 20 μL or 40 μL (using optional 40 μL

analytical head

Up to 600 bar using 100 μL (default) or

optional 40 μL analytical head

 

0.1 500 μL or 900 μL in 0.1 μL increments (using

900 μL analytical head)

Pressure range up to 400 bar due to 900 μL

analytical head

 

0.1 120 μL in 0.1 μL increments with 1290

Infinity large volume injection kit (hardware

modification required) G4216-68711

0.1 500 μL or 1500 μL in 0.1 μL increments with

100 μL upgrade kit (hardware modification

required) G7167-68711

Pressure range up to 600 bar Multi-draw

modus (Injection into needle-seat capillary)

Injection range for

Dual-needle

instruments

Default: 0.1 100 μL in 0.1 μL increments;

optional: 20 μL or 40 μL (using 100 μL analytical

head)

Up to 600 bar using 100 μL analytical head

 

Up to 900 μL in 0.1 μL increments depending on

installed loop size

Up to 600 bar using 100 μL analytical head

Precision for

Single-needle

instruments

<0.15 % RSD or SD <10 nL, whatever is greater

Measured caffeine

Precision for

Dual-needle

instruments

<0.2 % RSD or SD <10 nL, whatever is greater

Measured caffeine

Pressure range

Up to 600 bar (G7167A)

Max pressure for basic instrument

Sample viscosity

range

0.2 5 cp

 

Sample capacity

1H Drawer up to 8 drawers and 16 positions

Shallow well plates (MTP)

Max. 6144/1536 samples (384MTP/96)

 

2H Drawer up to 4 drawers and 8 positions

MTP, deep well plates, vials, Eppendorf

3072 samples, 432 vials (2 mL)

 

3H Drawer up to 2 drawers and 4 positions

MTP, deep well plates, vials up to 6 mL,

Eppendorf

1536 samples, 60 vials (6 mL), 384 vials

(1 mL), 216 vials (2 mL)

Injection cycle time

<10 s using following standard conditions:

Default draw speed: 100 μL/min

Using standard Single-needle setup

 

Default eject speed: 400 μL/min Injection

volume: 1 μL

Time between 2 injections is not

mechanically limited, time delay depends on

communication speed of software, OS or

network connections

Carry Over

<0.003 % (30 ppm) Multisampler Standard and

Dual Needle

<0.0009 % (9 ppm) Multisampler Multiwash

Using the following conditions:

Column: Agilent Pursuit XRs 3 C18, 2.0 x

50 mm

Mobile phase:

A: 0.1 % TFA in water

B: 0.1 % TFA in Acetonitrile

Isocratic : % B=40 %

Flow rate: 0.5 mL/min

Temperature: 25 °C

Wavelength: 257 nm

Sample: 1200 ng/μL Chlorhexidine

(dissolved with mobile phase A), 1 μL

injected and measured on G4212A DAD

Wash solution: H2O with 0.1 % TFA (3 s)

Multiwash

Outer needle wash and seat backflush for

carryover reduction with up to 3 different

solvents

 

Control and data

evaluation

Agilent Open Lab CDS

A.02.01 or above (A.02.02 supports Sample

Entry UI)

 

MassHunter QQQ

B.07.00 SP11 or above

 

MassHunter QTOF

B.05.01 SP31 or above

 

Lab Advisor

B.02.05 or above

 

ICF for 3rd party SW control

A.02.01 or above

 

LC and CE Drivers

A.02.10 or above

Local Control

Agilent Instant Pilot (G4208A)

B.02.17 or above (currently not

supported/official release 2015)

Communications

Controller-area network (CAN), Local Area

Network (LAN)

ERI: ready, start, stop and shut-down signals

 

Safety and

maintenance

Extensive support for troubleshooting and

maintenance is provided by the Instant Pilot,

Agilent Lab Advisor, and the Chromatography

Data System.

Safety-related features are leak detection, safe

leak handling, leak output signal for shutdown of

pumping system, and low voltages in major

maintenance areas

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage with

user-settable limits and feedback messages.

Electronic records of maintenance and errors.

 

Housing

All materials recyclable

 

Metering device

Metering device in high pressure flow path

 

 

 

Performance Specifications G5668A

Table 5 Agilent 1260 Infinity II Bio-inert Multisampler (G5668A) Performance Specifications

Type

Specification

Comment

Injection range

Default: 0.1 100 μL in 0.1 μL increments

Up to 600 bar using 100 μL

 

Default: 0.1 250 μL or 1000 μL in 0.1 μL

increments with Multidraw upgrade kit (Bio-inert)

(G5667-68711

Pressure range up to 400 bar Multi-draw

mode (Injection into needle-seat capillary)

Precision

<0.15 % RSD or SD <10 nL, whatever is greater

Measured caffeine

Pressure range

Up to 600 bar

Max pressure for basic instrument

Sample viscosity

range

0.2 5 cp

 

Sample capacity

1H Drawer up to 8 drawers and 16 positions

Shallow well plates (MTP)

Max. 6144/1536 samples (384MTP/96)

 

2H Drawer up to 4 drawers and 8 positions

MTP, deep well plates, vials, Eppendorf

3072 samples, 432 vials (2 mL)

 

3H Drawer up to 2 drawers and 4 positions

MTP, deep well plates, vials up to 6 mL,

Eppendorf

1536 samples, 60 vials (6 mL), 384 vials

(1 mL), 216 vials (2 mL)

Injection cycle time

<10 s using following standard conditions:

Default draw speed: 100 μL/min

Using standard Single-needle setup

 

Default eject speed: 400 μL/min Injection

volume: 1 μL

Time between 2 injections is not

mechanically limited, time delay depends on

communication speed of software, OS or

network connections

Carry Over

<0.003 % (30 ppm) Multisampler Standard

<0.0009 % (9 ppm) Multisampler Multiwash

Using the following conditions:

Column: Agilent Pursuit XRs 3 C18, 2.0 x

50 mm

Mobile phase:

A: 0.1 % TFA in water

B: 0.1 % TFA in Acetonitrile

Isocratic : % B=40 %

Flow rate: 0.5 mL/min

Temperature: ambient

Wavelength: 257 nm

Sample: 1200 ng/μL Chlorhexidine

(dissolved with mobile phase A), 1 μL

injected and measured on G4212A DAD

Wash solution: H2O with 0.1 % TFA (3 s)

Multiwash

Outer needle wash and seat backflush for

carryover reduction with up to 3 different

solvents

 

Materials in flow

path

Titanium, gold, PTFE, PEEK, ceramic

Upstream of sample-introduction

 

PEEK, ceramic

Downstream of sample-introduction

Control and data

evaluation

Agilent Open Lab CDS

A.02.01 or above (A.02.02 supports Sample

Entry UI)

 

MassHunter QQQ

B.07.00 SP11 or above

 

MassHunter QTOF

B.05.01 SP31 or above

 

Lab Advisor

B.02.05 or above

 

ICF for 3rd party SW control

A.02.01 or above

 

LC and CE Drivers

A.02.10 or above

Local Control

Agilent Instant Pilot (G4208A)

B.02.17 or above (currently not

supported/official release 2015)

Communications

Controller-area network (CAN), Local Area

Network (LAN), USB

ERI: ready, start, stop and shut-down signals

 

Safety and

maintenance

Extensive support for troubleshooting and

maintenance is provided by the Instant Pilot,

Agilent Lab Advisor, and the Chromatography

Data System.

Safety-related features are leak detection, safe

leak handling, leak output signal for shutdown of

pumping system, and low voltages in major

maintenance areas.

 

GLP features

Early maintenance feedback (EMF) for

continuous tracking of instrument usage with

user-settable limits and feedback messages.

Electronic records of maintenance and errors.

 

Housing

All materials recyclable.

 

Metering device

Metering device in high pressure flow path

 

 

Physical Specifications of the Sample Cooler

Table 6 Physical Specification of the Sample Cooler

Type

Specification

Comments

Weight

< 6 kg

 

Dimensions

(height × width × depth)

205 mm x 340 mm x 370 mm

 

Refrigerant gas

HFC-134a (0.042 kg)

Ozone depletion

potential (ODP) = 0

Supply voltage

24 VDC (nominal)

 

Current

10 A max.

 

Ambient operating temperature

4 40 ° C (39.2 104 ° F)

 

Ambient non-operating

temperature

-40 70 ° C (-20 158 ° F)

 

Operating altitude

Up to 3000 m (9842 ft)

 

Non-operating altitude

Up to 4600 m (15091 ft)

 

Safety standards:

IEC, EN, CSA, UL

Installation category II, Pollution

degree 2

For indoor use only.

ISM Classification

ISM Group 1 Class B

According to CISPR 11

Table 7 Performance Specifications Agilent 1290 Sample Cooler

Type

Specifications

Operating principle

High performance, low-energy consumption

micro-compressor based cooler with

ozone-friendly HFC-134a coolant (42 g),

user-upgradable.

Temperature range

from 4 °C to 5 °C below ambient

Temperature settable

from 4 40 °C in 1 ° increments

Temperature accuracy (<25 °C, <50 % r.H.)

2 °C to 6 °C at a setpoint of 4 °C

 

 

 

3
配置

 

NOS.

Parts No.

Description

1

G7110B  1260 Infinity II等度泵(最大压力 600 bar。包括等度泵 、色谱柱、连接毛细管、溶剂柜、溶剂瓶和 CAN 电缆。)

1260 Infinity II Quaternary Pump

2

G7110B  001  液相工具包(液相色谱系统工具包。包括运行和维护安捷伦 1200 Infinity 系列液相色 谱系统所需要的工具。)

HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC

3

G7110B  032 主动阀套件

Active Inlet Valve (AIV)

4

G7110B 030 泵头密封垫清洗装置

Active Seal Wash

5

G1328C  1260 Infinity 手动进样器。包括 600 bar 的手动进样阀、 20 μL样品瓶和固定支架。

1260 Series Manual Injector. Includes Rheodyne 7725 manual injection valve, 20 ul sample loop and mounting stand.

6

G7111A  1260 Infinity II四元梯度泵含在线脱气机(四元泵。最大压力 400 bar。包括内置的四通道脱气单元。包括四元泵、连接毛细管、溶剂柜和 CAN 电缆。)

1260 Infinity II Quaternary Pump VL, maximum pressure 400bar. Includes quaternary pump, column, connecting capillaries, solvent cabinet, solvent bottles and CAN cable.

7

G7111A  001  液相工具包(液相色谱系统工具包。包括运行和维护安捷伦 1200 Infinity 系列液相色 谱系统所需要的工具。)

HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC

8

G7111A 032 主动阀套件

Active Inlet Valve (AIV)

9

G7111A 030 泵头密封垫清洗装置

Active Seal Wash

10

G7111B  1260 Infinity II四元梯度泵含在线脱气机(1260 Infinity II 四元泵,最大压力 600 bar。包括四元泵 、连接毛细管、溶剂柜、溶剂瓶和 CAN 电缆。)

1260 Infinity II Quaternary Pump VL, maximum pressure 600bar. Includes quaternary pump, column, connecting capillaries, solvent cabinet, solvent bottles and CAN cable.

11

G7111B  001  液相工具包(液相色谱系统工具包。包括运行和维护安捷伦 1200 Infinity 系列液相色 谱系统所需要的工具。)

HPLC System Tool Kit, for Agilent 1260/1290 Infinity II LC

12

G7111B 032 主动阀套件

Active Inlet Valve (AIV)

13

G7111B 030 泵头密封垫清洗装置

Active Seal Wash

14

G7111B 093 色谱柱

Agilent Poroshell 120 EC-C18 4.6x100mm, 2.7um

15

G7122A 1260 Infi nity II 脱气机

1260 Infi nity II Degasser 4 channels; up to 10 mL/min fl ow; 12mL internal volume per channel

16

G7129A 1260 Infinity II 样品瓶进样器                                            (1260 Infinity II 样品瓶进样器,耐压高达 600 bar。包括  100 μL 的计量装置以及 100 μL 的样品定量环,带集成进样针清洗口 。包括 2 个抽屉,每个抽屉可容纳 66 个样品瓶 (2 mL)

1260 Infinity II Vialsampler for use up to 600 bar. Includes 100 uL metering device and a 100 uL sample loop plus integrated needle flush port. Includes 2 drawers each for 66 vials (2 mL).

17

G7167-60005 温控器

Infinity II Sample Cooler

18

G7129A 1260 ICC 063集成式柱温箱 可容纳 2 根色谱柱,加热体积 6 μL)

1260 Thermostatted Column Compartment

19

G7116A 1260 Infinity II 高容量柱温箱 可容纳 2 根色谱柱,加热体积 7 μL)

10 degrees below ambient to 85 °C; up to four 30 cm columns; up to four individual

Infi nityLab Quick-Connect heat exchangers; optional valve drive for Infi nityLab Quick

Change valve heads (up to 600 bar and up to 4-column selection without re-plumbing)

20

G7167A 1260 Infinity II Multisampler,耐压高达 600 bar,用于孔板和单个样品容器。包括 2 个样品抽屉、2 54 样品瓶容器 、一个进样针清洗口、100 μL 计量装置和样品定量环。

1260 Infinity II Multisampler

21

G7117C 1260 Infinity II 二极管阵列检测器 HS。适用于超高灵敏度的快 速多波长光谱分析。数据采集速率最高达 120 Hz。用于流通池和灯的 RFID  标签。包括 10 mm 标准最大光强卡套式流通池,体积 1 μL

5410是专为快速离心少量样品而设计的。外形精巧,运行时声音极低,具备离心机所需性能:Short- spin 瞬时离心功能.

22

G7121A  1260 Infinity II 荧光检测器(适用于可编程单波长检测(激发和发 射),数据采集速率高达 74 Hz。包括标准流通池,8μL

1260 Infinity II Variable Wavelength Detector

23

G7121B  1260 Infinity II 荧光检测器(适用于多波长检测,可在线采集 激发和发射光谱,采集速率最高达 148 Hz。包括标准流通池,8μL

1260 Infinity II Variable Wavelength Detector

24

G7162A 1260 Infinity II 示差折光检测器。数据采集速率最高达 72 H z,配备集成式 8 μL 标准流通池

1260 Infinity II Refractive Index Detector

25

G4260B  蒸发光散射检测器

Agilent 1260 Infinity ELSD

26

ELSD模拟输出电缆线

38x-ELSD Analogue Output Cable

27

M8301AA 工作站数据处理系统

OpenLAB CDS ChemStation Workstation

28

M8500AA 工作站采样系统

OpenLAB CDS Inst. Driver for Agilent LC

29

M8410AA  OpenLAB CDS 工作站软件

 

30

M8410AA         001

液相色谱仪连接许可

 

31

M8410AA         005

3D UV/DAD 连接许可

 

32

5063-6591  手拧PEEK接头,1/16英寸,10/

PEEK finger-tight 1/16 in, 10PK

33

0890-1763  PEEK

1/16"od 0.007"id (0.18mm) 1.5m PEEK tbng

34

8710-1930 塑料管线切割器

Plastic and PEEK tubing cutter

35

5182-0714  2mL广口螺纹口玻璃瓶、透明,100/

Vial,screw,2ml,clr,cert,100PK

36

5182-0727  广口,无隔垫螺纹口瓶盖,用于2 mL 样品瓶,100/

Green color screw caps  100/PK

37

5182-0731  PTFE/红色硅橡胶乳白色隔垫,100/

Septa, PTFE/red silicone, 8.7mm 100/pk

38

5063-6589 柱塞杆密封垫,石墨填充的PTFE(反相),(G1310AG1311AG1312AG1376AG2226A11201220G1310BG1311BG1312BG1311CG1312CG4303A

Plunger seal for 1100/1200 and 1050 2/PK

39

01018-22707 过滤白头,5/

PTFE Frits 5PK

40

01018-60025

Solvent inlet filter, stainless steel

41

693970-902T 分析型液相色谱住,带色谱柱 IDInfinityLab Poroshell 120 色谱柱可在主流液相色谱系统压力范围内实现稳定的高分离度分离,分析速度最高可比传统 5µm 方法快 5 倍)

InfinityLab Poroshell 120 EC-C184.6×150 mm4μm

42

990967-902 XDB-C18色谱柱      (温度上限:60℃, pH :2.0-9.0

XDB-C18 Analytical HPLC Col 4.6 x250

43

820950-925 保护柱芯,4/

Eclipse XDB-C18 4.6x12.5,5u Grd Car 4/PK

44

820999-901 保护柱卡套

High Perf. ZORBAX Guard Fittings Kit

45

SYS-LC-1260

硬件认证

LC 1260 System

46

SYS-LC-1260     6N9

硬件IQ认证  (安装验证)

Enterprise Qualification IQ

47

SYS-LC-1260     6J9

硬件OQ认证(操作验证)

Enterprise Qualification OQ                                                                                                                       企业版操作认证

48

SYS-SW-OLAB-E

软件认证

OpenLAB CDS WorkStation

49

 

 

50

SYS-SW-OLAB-E   6N9

软件IQ认证(安装验证)

Enterprise Qualification IQ

51

SYS-SW-OLAB-E   6J9

软件OQ认证(操作验证)

Enterprise Qualification OQ

Type Specification Comments Weight 14.7 kg (32 lbs) Dimensions (height × width × depth) 180 x 396 x 436 mm (7.1 x 15.6 x 17.2 inches) Line voltage 100 – 240 V~, ± 10 % Wide-ranging capability Line frequency 50 or 60 Hz, ± 5 % Power consumption 80 VA, 65 W Ambient operating temperature 4–55 °C (39–131 °F) Ambient non-operating temperature -40 – 70 °C (-40 – 158 °F) Humidity < 95 % r.h. at 40 °C (104 °F) Non-condensing Operating altitude Up to 3000 m (9842 ft) Non-operating altitude Up to 4600 m (15092 ft) For storing the module Safety standards: IEC, EN, CSA, UL Installation category II, Pollution degree 2 For indoor use only. ISM Classification ISM Group 1 Class B According to CISPR 11

4
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